In the case of Marbury v. Madison, the Supreme Court:

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In the case of Marbury v. Madison, the Supreme Court declared a federal law (specifically, part of the Judiciary Act of 1789) unconstitutional. This was a significant decision, as it established the principle of judicial review, which gives the Supreme Court the power to determine the constitutionality of laws passed by Congress or actions taken by the executive branch. This decision solidified the role of the Supreme Court as a co-equal branch of government and helped to establish the balance of power between the three branches.

In the Case of Marbury V